To cmaffe:
In the past we carbon treated our acid copper plating baths
on a time basis as you are curently doing.About 10 years ago we switched from
a time accumulation basis to an amperage basis.We are currently carbon
treating when 600 Amp Hours/Gal.is reached.
The following factors were used to arrive at this number:
1.Plating distribution, surface:hole
2.Surface plating distribution,top of the top racked
panel:bottom of the bottom racked panel
3.Cross sections; grain structure and corner cracking
4.Ductility
5.Hull cell
These are Lea Ronal PCM+ baths with automatic brightner
dosig.All plating is pattern plate with Dynachem LP resist.The carbon treat
cycle uses an oxidizer followed by the carbon all done off line in a batch
process.This should provide you with a starting point.Obviously many factors
can influence your requirement;resist,chemisties-preclean/acid
copper,rinsing,carbon treat procedure,end user specifications etc.etc.
Regards
Michael Barmuta
Staff Engineer
Fluke Corp.
Everett Wa.
(206)356-6076
On Mon, 29 Jul 1996 07:06:29 -0700 [log in to unmask] wrote:
> From: [log in to unmask]> Date: Mon, 29 Jul 1996 07:06:29 -0700
> Subject: Carbon Treatment
> To: [log in to unmask]
> Cc: [log in to unmask], [log in to unmask], [log in to unmask]
>
> With higher tech product these days and the associated high aspect
> ratio copper plating chemistries, we're looking for a good method to
> determine when to carbon treat as a preventative measure. For years
> I've used a guideline of carbon treating copper baths every 6 mos. or,
> if through put per gal was very high, perhaps quarterly.
>
> T&E results are so susceptible to sample prep, and I've never really
> found them to correlate to anything but perhaps extreme organic
> contamination. I've never felt comfortable relying on those to
> indicate when to treat.
>
> Multiple thermal shock is another method I'm hearing is an indicator.
> We currently pass six or more, yet just went through a bath decant to
> minimize detrimental organic build up while awaiting installation of a
> new carbon treatment system. The baths are only about 6 mos. old but
> with only about 3 months of production throughput.
>
> Appreciate any ideas or schemes that work for others, especially high
> volume, high tech.
>
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