Frank,
Send the boards back to your supplier!!!
Lead is used as a stabiliser in Electroless Nickel baths but in the ppm
range!!
From your description it sounds like you have a problem with ENi becoming
passive - oxidising prior to gold application. This will give you the black
appearance and peeling gold. Too thin a gold may also be a problem which is
porous and allowed the Nickel to oxidise.
In short - at the very least do a solderability check and send them back!!
Russell
Atotech UK
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