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From: | |
Reply To: | DesignerCouncil E-Mail Forum. |
Date: | Thu, 19 Feb 1998 07:18:40 -0600 |
Content-Type: | text/plain |
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> I am looking for an adhesive with the following properties:
>
> 1. Capable of bonding kovar to sapphire.
> 2. Hermetic seal.=20
> 3. Thermal coefficient of expansion (TCE) of approximately 5.66
> x 10^-6 in/in /=B0C=20
> (0 to 100 =B0C range). =20
> 4. Translucent.
> 5. Fast curing, with no outgassing.
>
> I need to bond two sapphire windows to each side of a 2.5" kovar
> wheel.=20
> The kovar wheel has two gas filled chambers. One chamber is
> filled with carbon monoxide and the other with
> nitrogen.
>
> Since sapphire and kovar have similar thermal expansion
> coefficients (between 3.24 - 5.66 x 10^-6 in/in/=B0C),=20
> it would be ideal if the adhesive also had a low thermal
> coefficient of expansion.
>
> The completed wheel assembly will be rotated at 1800 rpm under
> very little vibration.=20
>
> Below is a drawing of what I would like to build. Thank you in
> advance for your consideration.
> =20
> Ron Hom
> Advanced Pollution Instrumentation, Inc.
The only suggestion I can up with dosen't involve adhesives. Many
years ago I bonded sapphire to kovar using a glass frit, and then
firing it. I made a slurry of powdered glass (can't remember the grade
number) and acetone, placed the sapphire lens on the kovar base, and
introduced the slurry around the seam using a fine artists brush.
Capillary action pulled the frit between the kovar and lens. This
was followed by firing the entire assembly in a high temperature
oven.
Tom Hybiske
General Atronics Corp.
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