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From [log in to unmask] Wed May 15 17: |
55:31 1996 |
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Hi Suzanne -
I have had white residue problems similar to yours but under
different circumstances. We found white residue on the pads/solder
fillets after a saponified water wash. The soldering process was RMA
wave flux, no nitrogen, wave solder process. The white residue was NOT
saponifier (we were using an Alpha product, basically a soap). We
found (after an enormously long investigation) that the white residue
was due to high water wash temperatures (greater than 150 F). We were
getting some type of lead - wash temperature reaction, most likely
related to the saponifier chemistry also, due to a run away heater.
The problem was corrected by replacing the heaters and improving the
temperature controls. You are using a different cleaning system than
we did but you may want to check out the temperature issues.
Dave Hillman
Rockwell Collins
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______________________________ Reply Separator _________________________________
Subject: White residue/lead oxide
Author: [log in to unmask] at ccmgw1
Date: 5/7/96 12:16 PM
We have a white residue problem at another division that has been analyzed
using FTIR and SEM EDAX that has shown it to be lead oxide. The white residue
is located on pads/solder fillets. The following process is used:
a. Yokota flow solder (preheat 220F topside, 495F solder pot (less than 3
seconds), conveyor speed 3.5 ft/min)
b. Kester 197 foam fluxer (rma)
c. Cleaner is Bioact EC7R in a Ney spray under immersion or ECD batch
diswasher. Temperature of EC7R 90-95F, Rinse waters 130F.
The white residue is observed after cleaning and is insoluble in alcohol
water/EC7R.
Any input on things to look for would be greatly appreciated. We are running
tests at other divisions with different flux chemistries/board design/process
parameters.
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