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August 2009

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Subject:
From:
Graham Naisbitt <[log in to unmask]>
Reply To:
TechNet E-Mail Forum <[log in to unmask]>, Graham Naisbitt <[log in to unmask]>
Date:
Mon, 24 Aug 2009 11:58:20 +0100
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text/plain (245 lines)
Ah ha!

So it would seem that the coating is soaking into the board surface  
which might suggest a resist starvation?

If you can, try a brush coat from "pure" material and see if the same  
condition recurs.

Aerosols generally speaking have ***all solids in them often less than  
5% - and its an expensive packaging medium - which is why I always  
recommend hand spraying if spraying is your preferred/required  
application method (dipping is bestest!) - Hand spray should allow you  
to get up around 20%+ solids from dipping which is at full strength  
~35-40% (1B31). Consequently aerosols might exhibit "poor coating"  
finishes more readily - because there's ***all there to begin with.

Let me know

Regards

Graham Naisbitt

Email: [log in to unmask]
Phone: +44 (0)12 5252 1500
Web: www.gen3systems.com

On 23 Aug 2009, at 20:06, Inge wrote:

> Yes, variations with same cans.
> OK, will try baking.
> Yes, from same fabricator.
> Mystery.
>
> One of our old foxes, experienced process engineer, you've met him,  
> made a try,
> At first, the wet coating was crystal clear, but successively  
> throughout room drying, the
> coating changed character, and became matte.
>
> Will let you know.
>
> Inge
>
>
>
> ----- Original Message ----- From: "Graham Naisbitt" <[log in to unmask] 
> >
> To: <[log in to unmask]>
> Sent: Sunday, August 23, 2009 6:35 PM
> Subject: Re: [TN] Manual spraying
>
>
>> Inge
>>
>> All from the same can?
>>
>> If no, then I suspect some incomplete curing or "residual board  
>> contaminants" might be the problem.
>>
>> Try baking the problem boards for around 8 hours at 80C, leave them  
>> to revert to room temp and try again. If problem persists, then  
>> there you probably need to run FTIR to figure what is there causing  
>> the problem.
>>
>> Also, are they from the same board fabricator? If not, check ROSE  
>> to  see if there is a difference.
>>
>> If yes, then have the batch checked - it is possible that there  
>> has  been a labelling issue.
>>
>> Let me know
>>
>> Regards
>>
>> Graham Naisbitt
>>
>> Email: [log in to unmask]
>> Phone: +44 (0)12 5252 1500
>> Web: www.gen3systems.com
>>
>> On 21 Aug 2009, at 12:48, Hernefjord Ingemar wrote:
>>
>>> Nick,
>>> we have done tests today, same operator, same boards, same cans,   
>>> same everything. Most boards get a clear, deep and nice look, but   
>>> suddenly we get a greyish coating, quite matte!
>>>
>>> Q1: what spray angle do you recommend?
>>> Q2: what spray pattern do you recommend? Zig-zag, up-and-down,  
>>> side- to-side or what?
>>> Q3: is the room RH of importance?
>>> Q4: is the process sensitive to laminar flow and if so, what  
>>> level  is critical?
>>>
>>> Inge
>>>
>>>
>>>
>>>
>>> -----Original Message-----
>>> From: TechNet [mailto:[log in to unmask]] On Behalf Of Nicholas  
>>> Redgrave-Plumb
>>> Sent: fredag 21 augusti 2009 12:31
>>> To: [log in to unmask]
>>> Subject: Re: [TN] Manual spraying
>>>
>>> The only way I can see for the propellant causing this kind of   
>>> problem is if the nozzle of the spray can is too close to the   
>>> substrate whilst spraying. I note several suggestions in the  
>>> posted  responses of expensive elevated IR curing ovens etc. for  
>>> IB31 but  these are really not necessary as this material is dry  
>>> to the  touch/"tack" dry in only minutes, dry in 24 hours and  
>>> cured/fully  optimised in 7 days. This would undoubtedly be  
>>> accelerated by an  elevated cure but it shouldn't really be  
>>> necessary. So all you  should really need is simple drying cabinet  
>>> at ambient temperature  just to take the solvent vapours away.
>>>
>>> Otherwise, it could be "champagning" or "solvent-popping" which  
>>> are terms to describe a condition where the surface of the  
>>> coating  material partially cures leaving solvent still trapped  
>>> inside the  wet- film. The solvent has to go somewhere so it finds  
>>> it's way out  through the surface and in doing so makes multiple  
>>> small holes.
>>>
>>> To avoid this problem should be a matter of going back to basics.
>>> Review the coating procedure, make sure the operators are properly  
>>> trained (and not getting the spray nozzle too close to the  
>>> substrate).
>>> If the volumes justify the use of a purpose-built spray booth for  
>>> conformal coating with intrinsic safety features and laminar air-  
>>> flow/ extraction then it might be worth going in that direction.
>>>
>>> But there should be a simple solution to this problem because the   
>>> usage of HumiSeal 1B31 globally, in both liquid and aerosol cans  
>>> is  massive.
>>>
>>> Nick Plumb
>>> Gen3 Systems Limited
>>> Farnborough, United Kingdom
>>>
>>> _________________________________
>>>
>>>
>>> On 20 Aug 2009, at 19:17, Inge wrote:
>>>
>>>> Good Evening,
>>>> we use small cans filled with 1B1 conformal coating for  
>>>> handspraying
>>>> boards. The guys are not satisfied with the result, because  
>>>> sometimes
>>>> the result is matte. Microscope photos show thousands of  
>>>> microscopic
>>>> bubbles in the coating. I suspect that it's included driving gas.  
>>>> Or
>>>> wrong handling the spray can.Anyone out there with experience?  
>>>> How do
>>>> you avoid this problem?
>>>> /Inge
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