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March 2005

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Subject:
From:
Brian Ellis <[log in to unmask]>
Reply To:
TechNet E-Mail Forum <[log in to unmask]>, Brian Ellis <[log in to unmask]>
Date:
Thu, 3 Mar 2005 12:26:52 +0200
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This is an established test, not for reliability, but to determine 
whether solder mask or conformal coating will vesicate. It has been in 
use for decades and is well established in literature. For ex., 
Tautscher mentions it on p. 10-31 of his book (1976) and cites 
MIL-STD-810 method 507 procedure 1:
2 hours at 115°C ±5°C, 15 psi ±5 psi followed by 1 hour at 125°C ±5°C, 
25 psi ±5 psi. He calls it the "autoclave test".

In my book (1986), on p. 290, section 26.2, I suggest using a domestic 
pressure cooker for 2 - 4 hours and examining it with a 10x magnifier 
for signs of vesication. On p. 138, I explain the mechanism of 
vesication, with a photo of a circuit on p. 140 (Fig. 13.5) with bad 
vesication after a pressure-cooker test.

So, yes, this test has been around for a long time and is very useful to 
determine that the adhesion of coatings is good, having been put over 
poorly cleaned products. I would say that this test is an absolute must 
when applying conformal coatings over "no-clean" flux residues. That 
having been said, 72 hours seems somewhat exaggerated, unless you are 
seeking potential delamination of inner layers.

Brian

Glynn Shaw wrote:
> Customer is taking fully loaded, tested assemblies and cooking them:
> 
> 2 atmospheres, absolute
> 121 deg C
> 100% humidity
> 72 hours
> 
> 
> Pass-fail criteria: boards must appear cosmetically identical, before and
> after cooking.
> 
> They don't... but the circuits aren't falling off the bones and the boards
> still function electrically after drying :-)
> 
> Question: is this a valid/known Jedec, IPC, or Telecom test or is customer
> using grandma's recipe? End use is cell phones.
> 
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