John,
All of these techniques at predicated by separation. I am looking for a technique that is general and does not require separation. A binary answer - yes or no.
Bev
----- Original Message -----
From: Sharp, John [mailto:[log in to unmask]]
Sent: Thursday, March 08, 2012 06:16 PM
To: [log in to unmask] <[log in to unmask]>
Subject: Re: [CN] Testing for Phthalates
Bev,
I make no claims as to being an expert in lab techniques. You are far
ahead of me on this.
But I remembered that when we were working on the IPC-1065 PCB Material
Declaration Guidelines, we listed analytical methods for many different
compounds and compound groups. In general, we used SW-846 methods, and
for phthalates we listed 3640A (Gel Permeation Cleanup) followed by
either:
* 8061A (GC with Electron Capture Detection),
* 8270C (Semivolatiles by GC/MS), or
* 8410 (GC/Fourier Transform- Infrared Spectrometry).
Sorry I can't be more helpful on this. Take care,
John Sharp | Corporate Product Compliance Manager | TriQuint
Semiconductor, Inc.
2300 NE Brookwood Parkway | Hillsboro, OR 97124 | *: 503-615-9712 |
Fax: 503-615-8902 | *: [log in to unmask]
***The information contained in this e-mail and any accompanying
attachment is confidential. If you are not the intended recipient or an
authorized agent of the intended recipient, and/or you have received
this e-mail through inadvertent error, then any disclosure,
dissemination, distribution, copying, further review or other use of the
contents of this e-mail and/or any attachment is prohibited. If you are
not the intended recipient or an authorized agent thereof, and/or you
have received this e-mail in error, please notify me immediately via
e-mail or by telephone at the phone number set forth above and destroy
this e-mail. Thank you.***
-----Original Message-----
From: ComplianceNet [mailto:[log in to unmask]] On Behalf Of Bev
Christian
Sent: Thursday, March 08, 2012 1:18 PM
To: [log in to unmask]
Subject: [CN] Testing for Phthalates
We test for the REACH restricted phthalates. Now I hear they might add
di-n-pentyl phthalate. My question to you all is:
Does anyone know of a general chemical test for phthalates? We have
tried FTIR and have got false positives and false negatives. I was
wondering if there was some wet chemistry test that could be used. I
figure sooner or later they are going to ban all of them so I would just
like to know if there are any in the materials I test, whether or not
they are already on a target list.
Bev Christian, PhD, Director,
Materials Interconnect Research - Product Quality
Research In Motion Limited
-----Original Message-----
From: ComplianceNet [mailto:[log in to unmask]] On Behalf Of Sharp,
John
Sent: Thursday, March 08, 2012 2:04 PM
To: [log in to unmask]
Subject: [CN] New WTO TBT Notifications - RoHS Exemptions for Pb & Cd
AND RF Spectrum for short-range devices
Hello ANSI Chemical Listers and IPC ComplianceNetters,
Attached are a couple of new WTO TBT Notifications. The new exemptions
for Pb and Cd are a little old, but are just being submitted to the WTO.
The other concerns the RF spectrum for short-range devices in the EU.
Other notifications are listed in the table at the bottom of this email,
in case you are interested.
Take care,
John Sharp | Corporate Product Compliance Manager | TriQuint
Semiconductor, Inc.
2300 NE Brookwood Parkway | Hillsboro, OR 97124 | (: 503-615-9712 |
Fax: 503-615-8902 | *: [log in to unmask] <mailto:[log in to unmask]>
***The information contained in this e-mail and any accompanying
attachment is confidential. If you are not the intended recipient or an
authorized agent of the intended recipient, and/or you have received
this e-mail through inadvertent error, then any disclosure,
dissemination, distribution, copying, further review or other use of the
contents of this e-mail and/or any attachment is prohibited. If you are
not the intended recipient or an authorized agent thereof, and/or you
have received this e-mail in error, please notify me immediately via
e-mail or by telephone at the phone number set forth above and destroy
this e-mail. Thank you.***
***********
Instructions for signing up to receive NIST alerts for WTO TBT
Notifications:
If you want to see them all, you can visit:
https://tsapps.nist.gov/notifyus/data/index/index.cfm. Once you are
registered, you can have these notices e-mailed to you.
******
New WTO TBT Notifications
Country
Notification
Date Issued
Final Date for Comments
Days Left to Comment
Products Covered
Full Text
Notifications posted in English by WTO on 3/7/2012:
<https://tsapps.nist.gov/notifyus/data/tbt/tbt.cfm?country_ID=D%2E0%3B%5
F%5E%28%2EB6PH0BM%2DX%3F%2D%3B%26P5%5D%2AV9%22K%3F%3FE%3A%20QETSP%3A%25I
%27%5D%3C6%5FS%5E%0A&issuedYear=%24%2FE%3F%5E%5FP%20%20%0A>
China
CHN/886
<https://tsapps.nist.gov/notifyus/data/notification/notification.cfm?tbt
_ID=D%2EP%2AKJ%28%26N%22EL0B%5D8K%28%3D%3A7R%20%40%3FV%3COT%3F%5FA%3A%20
TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A>
3/2/2012
5/10/2012
63
Cosmetics
View full text CHN/886 (PDF)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?t
bt_ID=D%2EP%2AKJ%28%26N%22EL0B%5D8K%28%3D%3A7R%20%40%3FV%3COT%3F%5FA%3A%
20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO92A%24%21%21%29P%28
9M%3A8C%3CEU%21%3D%40%28%3EJ%3C%5BE871%29AE%40%27%2AZ%26I%227%3A%22LK%3D
A%3BJY%29%5BW%3A%21L%0AA%3F%29F%29A%5D%26XA%3B%261V%3A%2AU%3FKF%5BF%26%3
A%27R%20N%3BE%3D%2A6%3FYBA%21%5CJQ%2F9F%21%0A&availAtCountry=%21%2F%20%2
0%20%0A>
<https://tsapps.nist.gov/notifyus/data/tbt/tbt.cfm?country_ID=D%2F0%3AI%
5E%5D3%5D7ET0BX0D%28%3D%3B%26P%25L7V9%23Z%2A%2F%5D%3A%21%24%40BRP%2E%2A%
5E%27Q%3E%22%3FW%5C%0A&issuedYear=%24%2FE%3F%5E%5FP%20%20%0A>
European Communities
EEC/364/Add.1
<https://tsapps.nist.gov/notifyus/data/corrigendum/corrigendum.cfm?corri
gendum_ID=D%2E%25%3F%5EJX6J%21EP0A8%24K%28%3D%3A7R%20%40%3FV%3COT%3F%5FA
%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A>
3/2/2012
Not given by country
0
Diesel engines installed in new agricultural tractors
View full text EEC/364/Add.1 (PDF) (ENGLISH)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?c
orrigendum_ID=D%2E%25%3F%5EJX6J%21EP0A8%24K%28%3D%3A7R%20%40%3FV%3COT%3F
%5FA%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO92A%24%21%2
1%29P%289M%3A8C%3CEU%21%3D%40%28%3EJ%3C%5BE871%29AE%40%27%2AZ%26I%227%3A
%22LK%3DA%3BJY%29%5BW%3A%21L%0AM%3F%29F%29A%5D%26%5EB%2BR1W%2BBK8%28%5EH
F%27%227AE2%2FEYOZ%3CI%2F%3A%23%2CJK%24IR%23LR%23MVXJG2%20J%26%40%3A%2C%
3A%0A%24%278%2E%29%3F0%20%20%0A&availAtCountry=%21%2F%20%20%20%0A>
<https://tsapps.nist.gov/notifyus/data/tbt/tbt.cfm?country_ID=D%2F0%3AI%
5E%5D3%5D7ET0BX0D%28%3D%3B%26P%25L7V9%23Z%2A%2F%5D%3A%21%24%40BRP%2E%2A%
5E%27Q%3E%22%3FW%5C%0A&issuedYear=%24%2FE%3F%5E%5FP%20%20%0A>
European Communities
EEC/365/Add.1
<https://tsapps.nist.gov/notifyus/data/corrigendum/corrigendum.cfm?corri
gendum_ID=D%2E%20%3B%5DKM%3AJ7%40%400A8%24K%28%3D%3A7R%20%40%3FV%3COT%3F
%5FA%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A>
3/2/2012
Not given by country
0
New Narrow Track Agricultural Tractors
View full text EEC/365/Add.1 (PDF) (ENGLISH)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?c
orrigendum_ID=D%2E%20%3B%5DKM%3AJ7%40%400A8%24K%28%3D%3A7R%20%40%3FV%3CO
T%3F%5FA%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO92A%24%
21%21%29P%289M%3A8C%3CEU%21%3D%40%28%3EJ%3C%5BE871%29AE%40%27%2AZ%26I%22
7%3A%22LK%3DA%3BJY%29%5BW%3A%21L%0AM%3F%29F%29A%5D%26%5EB%2BR1W%2BBK8%28
%5EHF%27%227AE2%2FEYOZ%3CI%2F%3A%23%2CJJ%24IR%23LR%23MVXJG2%20J%26%40%3A
%2C%3A%0A%24%278%2E%29%3F0%20%20%0A&availAtCountry=%21%2F%20%20%20%0A>
<https://tsapps.nist.gov/notifyus/data/tbt/tbt.cfm?country_ID=D%2F0%3AI%
5E%5D3%5D7ET0BX0D%28%3D%3B%26P%25L7V9%23Z%2A%2F%5D%3A%21%24%40BRP%2E%2A%
5E%27Q%3E%22%3FW%5C%0A&issuedYear=%24%2FE%3F%5E%5FP%20%20%0A>
European Communities
EEC/373/Add.1
<https://tsapps.nist.gov/notifyus/data/corrigendum/corrigendum.cfm?corri
gendum_ID=D%2FE%2EM%5D%2D%5FY7EH0A8%24K%28%3D%3A7R%20%40%3FV%3COT%3F%5FA
%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A>
3/2/2012
Not given by country
0
Electric and electronic equipment as defined under Article 3(a) of
Directive 2002/95/EC
View full text EEC/373/Add.1 (PDF) (ENGLISH)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?c
orrigendum_ID=D%2FE%2EM%5D%2D%5FY7EH0A8%24K%28%3D%3A7R%20%40%3FV%3COT%3F
%5FA%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO92A%24%21%2
1%29P%289M%3A8C%3CEU%21%3D%40%28%3EJ%3C%5BE871%29AE%40%27%2AZ%26I%227%3A
%22LK%3DA%3BJY%29%5BW%3A%21L%0AM%3F%29F%29A%5D%26%5EB%2BR1W%2BBK8%28%5EH
F%27%227AE2%2FEYOZ%3CI%2F%3A%23%2CNL%24IR%23LR%23MVXJG2%20J%26%40%3A%2C%
3A%0A%24%278%2E%29%3F0%20%20%0A&availAtCountry=%21%2F%20%20%20%0A>
<https://tsapps.nist.gov/notifyus/data/tbt/tbt.cfm?country_ID=D%2F0%3AI%
5E%5D3%5D7ET0BX0D%28%3D%3B%26P%25L7V9%23Z%2A%2F%5D%3A%21%24%40BRP%2E%2A%
5E%27Q%3E%22%3FW%5C%0A&issuedYear=%24%2FE%3F%5E%5FP%20%20%0A>
European Communities
EEC/399/Add.1
<https://tsapps.nist.gov/notifyus/data/corrigendum/corrigendum.cfm?corri
gendum_ID=D%2F%40%2B%5FJ83%5F70H0A8%24K%28%3D%3A7R%20%40%3FV%3COT%3F%5FA
%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A>
3/2/2012
Not given by country
0
Short-range devices
View full text EEC/399/Add.1 (PDF) (ENGLISH)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?c
orrigendum_ID=D%2F%40%2B%5FJ83%5F70H0A8%24K%28%3D%3A7R%20%40%3FV%3COT%3F
%5FA%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO92A%24%21%2
1%29P%289M%3A8C%3CEU%21%3D%40%28%3EJ%3C%5BE871%29AE%40%27%2AZ%26I%227%3A
%22LK%3DA%3BJY%29%5BW%3A%21L%0AM%3F%29F%29A%5D%26%5EB%2BR1W%2BBK8%28%5EH
F%27%227AE2%2FEYOZ%3CI%2F%3A%23%2C6F%24IR%23LR%23MVXJG2%20J%26%40%3A%2C%
3A%0A%24%278%2E%29%3F0%20%20%0A&availAtCountry=%21%2F%20%20%20%0A>
<https://tsapps.nist.gov/notifyus/data/tbt/tbt.cfm?country_ID=D%2F%406K%
5E8%2AO%220D0%40M0D%3EM%3B%26G0Q%2FV9%23Y%2A%2FU%3A%20%24%40FSE%276%5FG%
40%2F%20%2AJL%0A&issuedYear=%24%2FE%3F%5E%5FP%20%20%0A>
Israel
ISR/575
<https://tsapps.nist.gov/notifyus/data/notification/notification.cfm?tbt
_ID=D%2FE%27%5D%5D%3D2L%220T0BX%28K%28%3D%3A7R%20%40%3FV%3COT%3F%5FA%3A%
20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A>
3/2/2012
5/2/2012
55
Domestic electrical appliances (HS Chapters 84-85)
View full text ISR/575 (PDF) (HEBREW)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?t
bt_ID=D%2FE%27%5D%5D%3D2L%220T0BX%28K%28%3D%3A7R%20%40%3FV%3COT%3F%5FA%3
A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO92A%24%21%21%29P%
289M%3A8C%3CEU%21%3D%40%28%3EJ%3C%5BE871%29AE%40%27%2AZ%26I%227%3A%22LK%
3DA%3BJY%29%5BW%3A%21L%0AI%3F%29F%29A%5D%26RGJV1V%3A%2AU%3FKF%5BF%26%3A%
27R%20N%3BE%3D%2A%3C9%282L%22%2CFW%299B%25I1JKVL%26Y2P%20%20%0A&availAtC
ountry=%21%2F%20%20%20%0A>
<https://tsapps.nist.gov/notifyus/data/tbt/tbt.cfm?country_ID=D%3A0%2B%5
C%5E%5D%5EL70H0T%2D%24E%2A%3D%3B%26F%25H%3CV%3CC%5C%3EOE%3A%204ATR%25%3A
%21%5E2D%2E%22%3F%5F%5E%0A&issuedYear=%24%2FE%3F%5E%5FP%20%20%0A>
United States of America
USA/682/Corr.1
<https://tsapps.nist.gov/notifyus/data/corrigendum/corrigendum.cfm?corri
gendum_ID=D%3AE%5EIK%2D%26J%21PP0B%5D%3CK%28%3D%3A7R%20%40%3FV%3COT%3F%5
FA%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A>
3/2/2012
Not given by country
0
Distribution transformers (HS 8504.21-34)
View full text of USA/682/Corr.1 (HTM)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?c
orrigendum_ID=D%3AE%5EIK%2D%26J%21PP0B%5D%3CK%28%3D%3A7R%20%40%3FV%3COT%
3F%5FA%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO%3DVT%24%
24A%2AQ%2CEZ%3A93%3CGE98V%5C%5EI%3B%5B8%24%27%20U%5EF%24CUSS1%3F%22%3F%5
B%5D%5C%5C%3C%3E%5CL%5C0D%3A%3DM%0A0%3FX%274S%2C%5B%2A%5F%5D%2A%2DAN%5FN
%2F%28Z%5BD%20%20%20%0A&availAtCountry=%21%2F0%20%20%0A>
View full text of USA/682/Corr.1 (PDF)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?c
orrigendum_ID=D%3AE%5EIK%2D%26J%21PP0B%5D%3CK%28%3D%3A7R%20%40%3FV%3COT%
3F%5FA%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO%3DVT%24%
24A%2AQ%2CEZ%3A93%3CGE98V%5C%5EI%3B%5B8%24%27%20U%5EF%24CUSS1%3F%22%3F%5
B%5D%5C%5C%3C%3E%5CL%5C0D%3B%5D%5D%0A%2F%3D%2C%2B%29SL%5F%29X%2CR%27A%5E
%23W8H%2AI%0A&availAtCountry=%21%2F0%20%20%0A>
<https://tsapps.nist.gov/notifyus/data/tbt/tbt.cfm?country_ID=D%3A0%2B%5
C%5E%5D%5EL70H0T%2D%24E%2A%3D%3B%26F%25H%3CV%3CC%5C%3EOE%3A%204ATR%25%3A
%21%5E2D%2E%22%3F%5F%5E%0A&issuedYear=%24%2FE%3F%5E%5FP%20%20%0A>
United States of America
USA/684
<https://tsapps.nist.gov/notifyus/data/notification/notification.cfm?tbt
_ID=D%3BP%2AM%5EX%3AM75P0B%5D%3CK%28%3D%3A7R%20%40%3FV%3COT%3F%5FA%3A%20
TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A>
3/2/2012
Not given by country
0
Toy safety
View full text of USA/684 (HTM)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?t
bt_ID=D%3BP%2AM%5EX%3AM75P0B%5D%3CK%28%3D%3A7R%20%40%3FV%3COT%3F%5FA%3A%
20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO%3DVT%24%24A%2AQ%2C
EZ%3A93%3CGE98V%5C%5EI%3B%5B8%24%27%20U%5EF%24CUSS1%3F%22%3F%5B%5D%5C%5C
%3C%3E%5CL%5C6D%3A%3DM%0A0%3FX%274S%2C%5B%2A%5F%5D%2A%2DAN%5BI%2F%28Z%5B
D%20%20%20%0A&availAtCountry=%21%2F0%20%20%0A>
View full text of USA/684 (PDF)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?t
bt_ID=D%3BP%2AM%5EX%3AM75P0B%5D%3CK%28%3D%3A7R%20%40%3FV%3COT%3F%5FA%3A%
20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO%3DVT%24%24A%2AQ%2C
EZ%3A93%3CGE98V%5C%5EI%3B%5B8%24%27%20U%5EF%24CUSS1%3F%22%3F%5B%5D%5C%5C
%3C%3E%5CL%5C6D%3B%5D%5D%0A%2F%3D%2C%2B%29SL%5F%29X%2CR%27AN%3FW8H%2AI%0
A&availAtCountry=%21%2F0%20%20%0A>
<https://tsapps.nist.gov/notifyus/data/tbt/tbt.cfm?country_ID=D%3A0%2B%5
C%5E%5D%5EL70H0T%2D%24E%2A%3D%3B%26F%25H%3CV%3CC%5C%3EOE%3A%204ATR%25%3A
%21%5E2D%2E%22%3F%5F%5E%0A&issuedYear=%24%2FE%3F%5E%5FP%20%20%0A>
United States of America
USA/685
<https://tsapps.nist.gov/notifyus/data/notification/notification.cfm?tbt
_ID=D%2D%25%5EKK%2D%5EL%23%20H0B%5D8K%28%3D%3A7R%20%40%3FV%3COT%3F%5FA%3
A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A>
3/5/2012
5/24/2010
Expired
Meat and poultry products
View full text of USA/685 (HTM)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?t
bt_ID=D%2D%25%5EKK%2D%5EL%23%20H0B%5D8K%28%3D%3A7R%20%40%3FV%3COT%3F%5FA
%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO%3DVT%24%25I9W%
281V%3F%28%5F%3CF%25I%2DD%3DJ%5E%2CJ%40%277%25%2DRD%21%26%3CKRE%3C%22%3E
%23%5D%5BL8%3C%5CLL2C%2F8W%0A%23%3EIF6%0A&availAtCountry=%21%2F0%20%20%0
A>
View full text of USA/685 (PDF)
<https://tsapps.nist.gov/notifyus/data/global/access_full_text_url.cfm?t
bt_ID=D%2D%25%5EKK%2D%5EL%23%20H0B%5D8K%28%3D%3A7R%20%40%3FV%3COT%3F%5FA
%3A%20TTDQ%406%2A%5FB%24%2E%20%2FW%5C%0A&url=M9%21%2E%5BO%3DVT%24%25I9W%
281V%3F%28%5F%3CF%25I%2DD%3DJ%5E%2CJ%40%277%25%2DRD%21%26%3CKRE%3C%22%3E
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